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Hach ANATEL PAT700 Operator's Manual

Other manuals for ANATEL PAT700: User Manual, User Manual
Manual is about: total Organic Carbon Analyzer

Summary of ANATEL PAT700

  • Page 1

    Anatel pat700 on-line total organic carbon analyzer operator manual.

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    Published in the united states of america. Hach ultra p/n: fg7005002 edition 01, november 29, 2007 copyright © 2007 by hach ultra analytics, inc. All rights reserved. No part of the contents of this manual may be reproduced or transmitted in any form or by any means without the written permission of...

  • Page 5: Table of Contents

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – table of contents page i anatel operator manual table of contents chapter 1 before you begin 1.1 about this manual . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 1 1.2 anatel ® pat700 anal...

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    Page ii table of contents – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 chapter 3 startup 3.1 startup sequence . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 35 3.2 logging on and off . . . . . . . . . . . . . . ....

  • Page 7

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – table of contents page iii anatel operator manual 5.8 security . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 59 general tab . . . . . . . . . . . . . . . . . . . . . . . . ....

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    Page iv table of contents – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 chapter 7 alarms 7.1 alarm indication . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 103 7.2 alarm acknowledgement . . . . . . . . . . . . . ...

  • Page 9

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – table of contents page v anatel operator manual chapter 11 maintenance and troubleshooting 11.1 maintenance . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 129 uv detect technology . . ...

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    Page vi table of contents – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1.

  • Page 11: Chapter 1

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – before you begin page 1 anatel operator manual chapter 1 before you begin 1.1 about this manual this instruction manual explains how to install and operate the anatel ® pat700 total organic carbon analyzer. • this c...

  • Page 12

    Page 2 before you begin – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 a touch-screen interface provides access to all analyzer functions. The user interface consists of a home screen from which all user operations initiate. The home scree...

  • Page 13

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – before you begin page 3 anatel operator manual the reader/writer retrieves the data stored on the rfid tags located on the bottom of the standards bottles. The rfid reader/writers have antennas that emit radio waves...

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    Page 4 before you begin – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 • follow all procedures in return procedures, page 137 , before shipping the analyzer to a service center for repair or recalibration. • make sure the analyzer is prope...

  • Page 15

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – before you begin page 5 anatel operator manual this equipment has been tested and found to comply with the limits for a class b digital device, pursuant to part 15 of the fcc rules. These limits are designed to prov...

  • Page 16

    Page 6 before you begin – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 1.9 precautionary labels read all labels and tags attached to the analyzer. Personal injury or damage to the instrument could occur if not observed. A symbol, if presen...

  • Page 17

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – before you begin page 7 anatel operator manual 1.10 symbols and marks the pat700 total organic carbon analyzer complies with those parts of 21 cfr, part 11 concerning the collection, retention, access and retrieval ...

  • Page 18

    Page 8 before you begin – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 parts per billion (ppb). A term used to report trace chemical analyses. It refers to the concentration of the element or compound present within one billion parts of wa...

  • Page 19: Chapter 2

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – installation page 9 anatel operator manual chapter 2 installation danger tasks involving installation of this equipment have fire, electrical, and pressure related hazards associated with them. These tasks must only...

  • Page 20

    Page 10 installation – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 • hook the analyzer onto the mounting bracket and latch it into place using the twist latches. • an optional handle, attached to the analyzer, enables it to be moved from ...

  • Page 21

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – installation page 11 anatel operator manual figure 2-2 pat700 analyzer orientation mounting general considerations follow these guidelines when installing the analyzer: • locate the analyzer where it is accessible f...

  • Page 22

    Page 12 installation – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 mounting to a wall follow these guidelines and refer to figure 2-1 , figure 2-2 ,and figure 2-3 to mount the transmitter to a wall or other flat, rigid surface: • use 5/16...

  • Page 23

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – installation page 13 anatel operator manual • use four 5/16-inch u-bolts, two for each 2-inch pipe, and eight matching nuts, to mount the analyzer mounting bracket to two rigid instrument poles. Use u-bolts and nuts...

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    Page 14 installation – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 2.3 plumbing connections caution potential eye and/or burn hazard! The water inlet can rupture if water pressure is too high. Sample inlet pressure must not exceed 100 psi...

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    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – installation page 15 anatel operator manual figure 2-5 pat700 connection to isolation valve process piping water inlet water outlet isolation valve (customer-supplied) drain.

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    Page 16 installation – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 water inlet and outlet tubing connects to the 1/4” inlet (water in) and outlet (water out) 316 stainless steel compression fittings on the analyzer. See figure 2-6 . Insta...

  • Page 27

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – installation page 17 anatel operator manual 6) leak test the connections by slowly opening the upstream isolation valve to introduce water into the analyzer. Pulse the valve several times by opening and closing it, ...

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    Page 18 installation – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 figure 2-8 pat700 power supply and i/o wiring terminals power supply wiring warning potential property damage or electrical shock! Adhere to ground network requirements fo...

  • Page 29

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – installation page 19 anatel operator manual figure 2-9 pat700 power supply wiring terminals i/o wiring the analyzer has three 4-20 ma outputs, two discrete inputs, and four discrete outputs. Connect wiring to the co...

  • Page 30

    Page 20 installation – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 discrete inputs the analyzer has two discrete inputs. Wiring connects to terminals on connector block j24, as listed in table 2-4 . • discrete input 1 initiates toc analys...

  • Page 31

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – installation page 21 anatel operator manual • discrete output 3 reports a warning or failure condition. A low state indicates an error condition exists. A high state indicates no error conditions exist. • discrete o...

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    Page 22 installation – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 figure 2-10 pat700 power supply and i/o wiring terminals power supply wiring warning potential property damage or electrical shock! Adhere to ground network requirements f...

  • Page 33

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – installation page 23 anatel operator manual i/o wiring the analyzer has three 4-20 ma outputs, two discrete inputs, and four discrete outputs. 4-20 ma outputs the analyzer has three 4-20 ma outputs, as listed in tab...

  • Page 34

    Page 24 installation – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 discrete outputs the analyzer has four discrete outputs, as listed in table 2-9 and table 2-10 . • discrete output 1 is a toc alarm. The output reports the toc level as ab...

  • Page 35

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – installation page 25 anatel operator manual 2.6 serial ports the analyzer has the following serial ports: • a female rs-232 serial port for data acquisition and control via a host computer. • a male rs-232 serial po...

  • Page 36

    Page 26 installation – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 2.7 rs-232 commands commands consist of 2-character, ascii text mnemonics. Some commands require one or more arguments, each delimited by at least one space (ascii 32, 20 ...

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    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – installation page 27 anatel operator manual mode setup commands data read commands the data normally are displayed only in response to the “rd” command. If the “sa” command is sent, data will be displayed at the end...

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    Page 28 installation – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 where: data logger commands example: read command: “re” response: alarm time alarm code “21:38:15 code #27” “21:44:40 code #36” “21:49:05 code #36” “…” “…” example: read c...

  • Page 39

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – installation page 29 anatel operator manual example: read command: “lp” or “lp 2007 07 25 12 13 2007 07 25 16 00” read format: “lp” or “lp yyyy mm dd hh mm yyyy mm dd hh mm” response: example: read command: “el” res...

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    Page 30 installation – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 parameter setup command example: read command: “sy” response: “7 25 2007 20 33 31” write format: “sy mm dd yyyy hh mm ss” “sy 7 30 2007 12 30 25” 1. Flush time (hh:mm:ss) ...

  • Page 41

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – installation page 31 anatel operator manual example: read command: “hr” read format: “hh:mm:ss hh:mm:ss u u u u s u u u u u u u u u u u u hh:mm:ss u u f u u u u u u f” response: “00:01:00 00:00:00 50 0 1 1 sensor 0 ...

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    Page 32 installation – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 example: read command: “pc” response: example: read command: “ps” response: example: read command: “pt” response: “pc” show conductivity calibration history “ps” show syst...

  • Page 43

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – installation page 33 anatel operator manual example: read command: “pv” response: diagnostic commands example: read command: “rm” read format: “mode state” response: “0 0” “pv” show toc validation history “rm” get a...

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    Page 34 installation – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1.

  • Page 45: Chapter 3

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – startup page 35 anatel operator manual chapter 3 startup 3.1 startup sequence the analyzer goes through the following sequence on power up: 1) splash window: the splash window appears at startup while the system lau...

  • Page 46

    Page 36 startup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 auto logoff the analyzer logs the current user off after the user-defined period of time. • if the analyzer is displaying the home screen, the icon in the sliding toolbar chang...

  • Page 47

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – startup page 37 anatel operator manual figure 3-2 home screen with sliding toolbar open run mode icon allows you to change the operating mode of the analyzer. Touching the icon takes you to the run mode dialog box w...

  • Page 48

    Page 38 startup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 • if no user is signed on, the sign on icon is present. Touching the icon when no one is signed on causes the sign on dialog box to appear, so you may enter your user id and pa...

  • Page 49

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – startup page 39 anatel operator manual • temperature is the last temperature reading in “temperature: x.X °c” format or “temperature: x.X °f” format, depending on the temperature units selected in the setup dialog b...

  • Page 50

    Page 40 startup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 graph tab the graph tab displays past data values. In all modes except conductivity, the graph displays toc values. In conductivity mode, the graph displays averaged conductivi...

  • Page 51: Chapter 4

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – run modes page 41 anatel operator manual chapter 4 run modes 4.1 the analysis cycle an analysis cycle is comprised of a flush of the analysis cell, oxidation, and idle time (if the cycle time is greater than the com...

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    Page 42 run modes – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 4.2 accessing run modes to access run modes, follow these steps: 1) at the home screen, touch the 2) touch the run mode icon. 3) at the run mode dialog box, touch the radio b...

  • Page 53

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – run modes page 43 anatel operator manual sampling with pressure caution potential burst hazard! Do not exceed the maximum 100 psi (690k pa) sample pressure ratings. Note using the sample pump on a pressurized system...

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    Page 44 run modes – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 in conductivity mode, the analyzer starts by verifying that the uv lamp is off and the cell valve is open to flush the cell. The analyzer reports the current readings for con...

  • Page 55

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – run modes page 45 anatel operator manual 4.7 self clean mode to access self clean mode, touch the self clean icon to open the self clean setup dialog box. Timed checkbox allows you to select timed or manual self cle...

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    Page 46 run modes – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1.

  • Page 57: Chapter 5

    Page 47 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 chapter 5 setup 5.1 accessing the setup dialog box 1) at the home screen, touch the 2) touch the setup icon. 5.2 setup dialog box the setup dialog box allows you to navigate and ...

  • Page 58

    Page 48 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 general tab figure 5-2 toc setup dialog box, general tab flush time text box allows you to specify the amount of time to flush the cell prior to beginning a toc analysis. You may...

  • Page 59

    Page 49 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 • a high to low state transition on digital1 aborts the current operation and immediately runs a single toc analysis. The analysis runs to completion regardless of whether subseq...

  • Page 60

    Page 50 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 5.4 system the system icon allows you to modify system settings for the analyzer. General tab figure 5-4 system settings dialog box, general tab instrument name text box allows y...

  • Page 61

    Page 51 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 display tab figure 5-5 system settings dialog box, display tab set time icon allows you to specify the date and time to be used in the system. You may enter any valid date in “yy...

  • Page 62

    Page 52 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 sounds tab figure 5-6 system settings dialog box, sounds tab alarm, warning, stop error, and user feedback list boxes enable you to select the system sounds to be associated with...

  • Page 63

    Page 53 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 static subnet mask text box sets the subnet mask for the analyzer. You may specify a value of 0 to 255 for each octet. The default value is 255.255.255.0. Static gateway text box...

  • Page 64

    Page 54 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 the actual (uncompensated) conductivity limits are in accordance with the specifications set forth in the method “ water conductivity” of the usp 25–nf 20 (january 2002). The act...

  • Page 65

    Page 55 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 figure 5-9 analog outputs setup dialog box toc zero scale text box sets the toc reading that corresponds to the lowest output for the selected range. You may enter a value from 0...

  • Page 66

    Page 56 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 5.7 printer the printer icon allows you to configure the printer settings for the analyzer. You can independently configure the printing of analysis results and the frequency of ...

  • Page 67

    Page 57 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 to change the printer settings: 1) turn the printer power switch off. 2) restore power while pressing the online button. Release the button when a printout of the current setting...

  • Page 68

    Page 58 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 toc tab figure 5-10 printer dialog box, toc tab disabled, continuous, and percent change radio buttons determine how often an online toc reading will be printed. You may select d...

  • Page 69

    Page 59 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 conductivity tab figure 5-11 printer dialog box, conductivity tab disabled, timed, and percent change radio buttons determine how often an online conductivity reading will be pri...

  • Page 70

    Page 60 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 general tab figure 5-12 security settings dialog box, general tab enable security checkbox allows you to enable or disable the analyzer’s security system. When security is enable...

  • Page 71

    Page 61 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 filename text box contains the filename for the exported data file, which includes all settings, the data log, and the alarm log. The default file name is mmddyyyyhhmmss (month, ...

  • Page 72

    Page 62 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 users tab the users tab allows you to add, edit, or delete users of the analyzer. Up to 10 users can be configured for the analyzer. Administrator and factory users cannot be del...

  • Page 73

    Page 63 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 print security settings icon prints the user settings for all users except administrator and factory users. Return icon returns you to the setup dialog box and saves the changes....

  • Page 74

    Page 64 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 audit trail tab only administrator and factory users can access the audit trail. Any additions, modifications, or deletions to the analyzer configuration are noted by a keyword (...

  • Page 75

    Page 65 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 clear data log icon allows you to clear the audit trail. Before you clear the data log, you must first answer “yes” when the clear datalog dialog box appears. Filter icon opens t...

  • Page 76

    Page 66 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 figure 5-19 filter data dialog box from/to date and time range text box. Only audit trail entries that fall between the from and to date and time ranges are displayed in the audi...

  • Page 77

    Page 67 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 user must manually accept results and auto accept results radio buttons determine whether the outcome of the test are manually or automatically accepted. You may select user must...

  • Page 78

    Page 68 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 return to online mode checkbox tells the analyzer whether or not to return to online mode following the calibration. You may enable or disable (default) this option. When enabled...

  • Page 79

    Page 69 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 system suitability tab figure 5-23 bottle test setup dialog box, system suitability tab return to online mode checkbox enables the analyzer to return to the online mode following...

  • Page 80

    Page 70 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 current password allows you to type your current password. You may enter 5 to 15 alphanumeric or symbol characters. New password allows you to type your new password. The new pas...

  • Page 81

    Page 71 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 export oxidation buffers icon copies all oxidation buffers (up to five) to a connected usb flash drive. Before copying begins, the analyzer verifies that there is data to export ...

  • Page 82

    Page 72 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 the thermistor tab shows the read-only coefficient values for the thermistor. Return icon returns you to the setup dialog box and saves the changes. Any changes are noted in the ...

  • Page 83

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – setup page 73 anatel operator manual warning text box (read-only) allows you to view the factory-set value for the uv detect™ sensor output to be measured before a lamp is marginal. Failure text box (read-only) allo...

  • Page 84

    Page 74 setup – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 the algorithm tab shows the algorithms used for stabilization time, auto stabilization limit, and uv step time. These are factory-set values that are read-only. Return icon retur...

  • Page 85: Chapter 6

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – bottle mode page 75 anatel operator manual chapter 6 bottle mode 6.1 calibration and validation bottle mode allows you to perform calibration, validation, and system suitability test procedures on the pat700. Proper...

  • Page 86

    Page 76 bottle mode – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 conductivity calibration protocol perform a conductivity calibration according to the guidelines established in usp method . The procedure uses an nist-traceable calibrated...

  • Page 87

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – bottle mode page 77 anatel operator manual grab sample button takes you to the grab sample load bottles dialog box. See grab sample, page 93 . Excursion mode button takes you to the excursion mode dialog box. See ex...

  • Page 88

    Page 78 bottle mode – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 the recommended correlation coefficient, a user-accepted value (r 2 ), is 0.990 or greater. The calibration will be accepted if the r 2 value is 0.990 or greater and the pe...

  • Page 89

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – bottle mode page 79 anatel operator manual figure 6-4 custom setup dialog box bottle selection check boxes enable you to enable or disable the bottles to use in the test. The default setting is all three bottles che...

  • Page 90

    Page 80 bottle mode – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 5) to use default settings, touch the use default settings radio button in the toc calibration setup dialog box. To run any other configuration, touch the use custom settin...

  • Page 91

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – bottle mode page 81 anatel operator manual figure 6-6 review test setup dialog box • test setup text lists the bottles that are loaded, test completion actions, acceptance criteria, and, if applicable, schedule. • b...

  • Page 92

    Page 82 bottle mode – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 • c of a value text box allows you to enter the certified analysis value for the standard that is being used. • volume text box allows you to enter the volume of water, in ...

  • Page 93

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – bottle mode page 83 anatel operator manual figure 6-9 test running dialog box • after verifying the presence of the appropriate standards, the analyzer performs a temperature stabilization. After the temperature has...

  • Page 94

    Page 84 bottle mode – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 • summary text lists the results of the test. The results appear as they would appear on the printed report. • export icon takes you to the export dialog box, where you can...

  • Page 95

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – bottle mode page 85 anatel operator manual figure 6-12 run again dialog box • checkmark icon returns you to the beginning of the test. All previous data are discarded. • cancel icon takes you to the unload/replace b...

  • Page 96

    Page 86 bottle mode – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 7) touch the toolbar, or touch the bottles icon in the lower left corner of the screen. 8) touch the run standards button in the bottle mode dialog box. See figure 6-1, pag...

  • Page 97

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – bottle mode page 87 anatel operator manual 14) if the selection has been made to use the conductivity meter verification resistor, install the resistor onto the analyzer’s 9-pin printer/calibration port, as illustra...

  • Page 98

    Page 88 bottle mode – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 • start test icon reads the value of the resistor. The analyzer then converts this value to conductivity by taking the inverse of the resistance and multiplying it by the c...

  • Page 99

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – bottle mode page 89 anatel operator manual 6.7 toc validation caution potential puncture hazard! Contact with the exposed needle could cause serious injury. Use extreme care when installing and removing the sample b...

  • Page 100

    Page 90 bottle mode – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 figure 6-17 load bottles dialog box, toc validation • bottle positions graphics show you the order in which to install the bottles. • unlock icon energizes the bottle bay d...

  • Page 101

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – bottle mode page 91 anatel operator manual 6.8 system suitability test caution potential puncture hazard! Contact with the exposed needle could cause serious injury. Use extreme care when installing and removing the...

  • Page 102

    Page 92 bottle mode – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 • bottle positions graphics show you the order in which to install the bottles. • unlock icon energizes the bottle bay door lock for five seconds, allowing you to open the ...

  • Page 103

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – bottle mode page 93 anatel operator manual 6.9 grab sample caution potential puncture hazard! Contact with the exposed needle could cause serious injury. Use extreme care when installing and removing the sample bott...

  • Page 104

    Page 94 bottle mode – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 • back icon takes you to the bottle mode dialog box. • forward icon takes you to the grab sample setup dialog box. • cancel icon returns you to the previous dialog box. All...

  • Page 105

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – bottle mode page 95 anatel operator manual figure 6-21 grab sample test in progress dialog box 8) when the grab sample test in progress dialog box appears, the analyzer begins running the test. • upon starting the g...

  • Page 106

    Page 96 bottle mode – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 figure 6-23 export grab sample dialog box filename text box allows you to specify the filename for the exported data file. Exporting record no: x bar graph indicator displa...

  • Page 107

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – bottle mode page 97 anatel operator manual figure 6-24 excursion mode dialog box • excursion with validation button opens the excursion with validation load bottles dialog box. See figure 6-25 and follow the instruc...

  • Page 108

    Page 98 bottle mode – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 figure 6-25 excursion mode with validation, load bottles dialog box • bottle positions graphics show you the order in which to install the bottles. • unlock icon energizes ...

  • Page 109

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – bottle mode page 99 anatel operator manual • run now icon immediately draws a water sample from the online source into the excursion bottle and opens the bottle filling dialog box. See figure 6-27 . • done icon retu...

  • Page 110

    Page 100 bottle mode – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 the excursion sample dialog box displays the analyzer’s serial number, the date and time of the excursion, the toc value, and the oxidation curve filename. Export icon ope...

  • Page 111

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – bottle mode page 101 anatel operator manual • cancel icon returns you to the previous dialog box. All changes made in any of the dialog boxes are lost. 2) close the bottle bay door. 3) touch the forward icon. The ex...

  • Page 112

    Page 102 bottle mode – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1.

  • Page 113: Chapter 7

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – alarms page 103 anatel operator manual chapter 7 alarms 7.1 alarm indication the analyzer has two basic operational modes: on-line and bottle. On-line toc and conductivity are the two primary on-line modes (although...

  • Page 114

    Page 104 alarms – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 7.2 alarm acknowledgement 1) if an alarm occurs, at the home screen, touch the toolbar. 2) touch the alarms icon. The alarm acknowledge dialog box allows you to view, acknowled...

  • Page 115

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – alarms page 105 anatel operator manual 7.3 alarm details touching one of the alarms in the list produces the alarm details dialog box. See figure 7-3 . Figure 7-3 alarm details dialog box alarm time text label indic...

  • Page 116

    Page 106 alarms – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 error alarms errors occur any time one of the non-critical subsystems fail or a failure occurs from which the analyzer attempts to recover. The animation area flashes red to in...

  • Page 117

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – alarms page 107 anatel operator manual critical error alarms a critical error occurs any time the analyzer cannot function due to an error in the system. The error appears as a full-screen, flashing message. All ope...

  • Page 118

    Page 108 alarms – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 37 temp_low temperature out of range low. 38 temp_high temperature out of range high. 39 resist_low resistivity out of range low. 40 resist_high resistivity out of range high. ...

  • Page 119

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – alarms page 109 anatel operator manual 131 unabletostart4to20maoutputs analyzer cannot start 4-20 ma output test. 132 unabletostartpumptest analyzer cannot start pump test. 133 unabletostoppumptest analyzer cannot s...

  • Page 120

    Page 110 alarms – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 measurement alarms a measurement alarm condition occurs any time the measured toc exceeds the user- defined limit or conductivity exceeds the usp-defined alarm limit. When an a...

  • Page 121: Chapter 8

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – diagnostics page 111 anatel operator manual chapter 8 diagnostics 8.1 accessing the diagnostics dialog box • at the home screen, touch the diagnostics icon, or • touch the dual uv lamp status indicator in the lower ...

  • Page 122

    Page 112 diagnostics – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 lamp test icon turns on each lamp for 180 seconds and tests the uv output level using the uv detect diagnostics. See figure 8-2 . If you touch the lamp test icon, the curr...

  • Page 123

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – diagnostics page 113 anatel operator manual pat700 lamp replacement to replace a lamp, follow these steps: 1) touch the replace lamp icon. 2) select the lamp to be replaced. 3) touch “run wizard” to run the lamp rep...

  • Page 124

    Page 114 diagnostics – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 figure 8-4 diagnostics dialog box, test tab rs-232 test the rs-232 test icon allows you to test serial communication from the serial port by using the printer port as a re...

  • Page 125

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – diagnostics page 115 anatel operator manual digital i/o test the digital i/o test icon allows you to test digital i/o communication. See figure 8-6 . Before you perform the digital i/o test, make sure i/o wiring is ...

  • Page 126

    Page 116 diagnostics – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 figure 8-7 4-20 ma output test dialog box output 1, output 2, and output 3 icons have the same functionality for each output. Touching one of the icons sends a 4 ma signal...

  • Page 127

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – diagnostics page 117 anatel operator manual figure 8-8 plumbing test dialog box flow path selection drop down list box allows you to select from 12 pre-configured valve and pump combinations. You may select none (de...

  • Page 128

    Page 118 diagnostics – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 figure 8-9 select bottles to load dialog box, plumbing test caution potential puncture hazard! Contact with the exposed needle could cause serious injury. Use extreme care...

  • Page 129

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – diagnostics page 119 anatel operator manual figure 8-10 load bottles dialog box, plumbing test • bottle positions graphics show you the order in which to install the bottles. • unlock icon energizes the bottle bay d...

  • Page 130

    Page 120 diagnostics – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 6) if a test is chosen immediately, the analyzer asks if you wish to install a bottle. If yes is selected, the load bottles dialog box illustrates the appropriate port in ...

  • Page 131

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – diagnostics page 121 anatel operator manual figure 8-13 pump calibration dialog box test time text box indicates the time in seconds that is used for the test and calibration functions. The test time is always 30 se...

  • Page 132

    Page 122 diagnostics – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 figure 8-14 fan test dialog box 8.5 calibration dates tab use the calibration dates tab for viewing the last dates that toc calibration, conductivity calibration, and syst...

  • Page 133: Chapter 9

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – data review page 123 anatel operator manual chapter 9 data review 9.1 accessing the data review dialog box 1) at the home screen, touch the 2) touch the data review icon. Access to the data review dialog box may be ...

  • Page 134

    Page 124 data review – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 9.3 export data data are exported in formatted text. The export function sends data to the usb port. Due to driver constraints, the analyzer is not compatible with all usb...

  • Page 135

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – data review page 125 anatel operator manual 9.4 filter data data filtering allows you to select the type and range of data to display, export or print. Data can be filtered by test type, date range, or special range...

  • Page 136

    Page 126 data review – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1.

  • Page 137

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – signing on and off page 127 anatel operator manual chapter 10 signing on and off if security is enabled, to access configuration and analyzer parameters, you must log on the system. Use the password dialog box to lo...

  • Page 138

    Page 128 signing on and off – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 10.3 expired password upon successful sign on, the analyzer checks to see if the user’s password has expired. If it has, you are prompted to change your password. 1...

  • Page 139

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – maintenance and troubleshooting page 129 anatel operator manual chapter 11 maintenance and troubleshooting danger tasks involving maintenance and service of this equipment may have electrical shock, eye, and chemica...

  • Page 140

    Page 130 maintenance and troubleshooting – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 failed lamp indications when code 128 is produced, the analyzer lamp has failed and must be replaced. Code 128 indicates that the uv lamp has failed an...

  • Page 141

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – maintenance and troubleshooting page 131 anatel operator manual warning uv lamp related shock, eye/skin, ozone gas and burn hazards are possible if the uv lamp is powered while outside the equipment lamp holder. Ins...

  • Page 142

    Page 132 maintenance and troubleshooting – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 8) grasp the lamp module on the right and left side and squeeze the module locking clips to release the module from the manifold assembly. Pull straigh...

  • Page 143

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – maintenance and troubleshooting page 133 anatel operator manual 9) press and hold the lamp retaining clip to release the uv lamp. While pressing the lamp retaining clip, carefully withdraw the lamp from the lamp hol...

  • Page 144

    Page 134 maintenance and troubleshooting – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 12) reconnect the lamp power connectors by carefully reinserting the connectors and locking them in place by twisting the locking rings clockwise. 13) ...

  • Page 145

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – maintenance and troubleshooting page 135 anatel operator manual 11.2 water filter replacement caution burn and pressure hazard! Water is pressurized and may be hot (up to 95 °c [203 °f]). Protective eye wear is requ...

  • Page 146

    Page 136 maintenance and troubleshooting – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 11.3 troubleshooting the pat700 incorporates extended diagnostic and reporting facility to inform the user about the nature of a problem. Alarm codes, ...

  • Page 147

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – maintenance and troubleshooting page 137 anatel operator manual • the instrument’s serial number. • sample resistivity and temperature. • current and historical toc data. • current and historical alarm codes. • a se...

  • Page 148

    Page 138 maintenance and troubleshooting – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 note failure to purge the analyzer of all liquid, remove all process materials, and thoroughly clean the analyzer before returning it to hach ultra ana...

  • Page 149

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – maintenance and troubleshooting page 139 anatel operator manual to purge the pat700 of entrained water: 1) remove the analyzer from service and disconnect it from the water system. 2) with the analyzer inlet and out...

  • Page 150

    Page 140 maintenance and troubleshooting – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1.

  • Page 151: Appendix A: Specifications

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – specifications page 141 anatel operator manual appendix a: specifications pat700 specifications are subject to change without notice. Toc specifications operating range 0.5 to 2,000 ppb as carbon display resolution ...

  • Page 152

    Page 142 specifications – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 physical specifications uv lamps two, with uv detect technology interface/display color touch screen maximum altitude 4,000 m (13,125 ft) user i/o wiring three 3/4-inch...

  • Page 153

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – specifications page 143 anatel operator manual input/output specifications analog output specifications analog outputs three, opto-isolated variables toc, conductivity, and temperature range configurable over 4-20 m...

  • Page 154

    Page 144 specifications – pat700 total organic carbon analyzer operator manual anatel wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1.

  • Page 155: Appendix B Ce Conformance

    Wg m - 2 8 no vemb e r 20 07 - ed it io n 0 1 pat700 total organic carbon analyzer – ce conformance page 145 anatel operator manual appendix b ce conformance.

  • Page 158

    Global headquarters 6, route de compois c.P. 212 ch-1222 vesenaz, geneva, switzerland tel +41 (0)22 594 64 00 fax +41 (0)22 594 64 99 americas headquarters 481 california avenue grants pass, oregon 97526 usa tel 1 800 866 7889 / +1 541 472 6500 fax +1 541 472 6170 www.Hachultra.Com © 2007 hach ultra...